Article citation information:
Vakulenko, I., Grischenko, N., Vakulenko, L., Efremenko, V., Proiydak, S., Perkov, O. Structure and properties of the steel railway wheel disc after forced cooling. Scientific Journal of Silesian University of Technology. Series Transport. 2018, 98, 173-180. ISSN: 0209-3324. DOI: https://doi.org/10.20858/sjsutst.2018.98.16.
Igor VAKULENKO1,
Nikolajj GRISCHENKO2, Leonid VAKULENKO3,
Vasily EFREMENKO4, Svetlana PROIYDAK5, Oleg PERKOV6
STRUCTURE
AND PROPERTIES OF THE STEEL RAILWAY WHEEL DISC AFTER FORCED COOLING
Summary. The technological use of accelerated cooling makes it possible to improve the carbon steel properties of the all-rolled railway wheel disc. The properties’ complex depends on the temperature of the accelerated cooling termination. This is determined by the ratio of the carbon atoms emitted from the supersaturated solid solution to the crystal structure defects and dispersion strengthening from carbide phase particles. If the cooling stops at a temperature above 350°C, the decline rate of the strength properties increases. This is caused by the excessive softening effect of the solid solution breakdown and cementite spheroidization during the processes of dispersion hardening.
Keywords: strength, carbon steel, wheel disc, accelerated cooling, microstructure
1. INTRODUCTION
Increased
operational intensity of railway transport is accompanied by the entirely
justified severization of operational safety requirements. The railway wheel is
an important structural element of rolling stock. Reliability increases in the
operation of railway wheels can be achieved by increasing the property complex
of metal by alloying or using heat treatment technologies [1,2]. A disc with
the smallest thickness is subjected to complex loads during the wheel
operation. This imposes high demands on the property complex of the railway
wheel disc. Quite often, when manufacturing the solid-rolled railway wheels,
after accelerated cooling of the wheel rim [3], the disc is cooled in air. Developing
technical solutions for improving the property complex and, primarily, the
combination of strength and ductility characteristics of the metal disc is an
important scientific and technical challenge. The use of accelerated cooling of
the disc surface is a promising technological solution, which makes it possible
to increase the property complex and operational safety of railway wheels under
current conditions of increasing specific loads on the wheel set. In [4], the
principal possibility of disc thermal hardening by water cooling using
nozzle-type devices is shown. Research has indicated that, at a depth of 3-
2. RESEARCH MATERIAL
AND METHODOLOGY
The
material for this research was railway wheel steel with the following
composition: 0.56% C; 0.66% Si; 0.43% Mn; 0.003% S; 0.012% P; 0.10% Cr. The
processes of structural formation in the different layers of the disc were
simulated during accelerated cooling by changing the temperature of forced
cooling termination. Blanks in the form of rods with a diameter of
3. RESEARCH RESULTS AND DISCUSSION
Figure 1
shows changes in the steel properties due to the temperature of the accelerated
cooling termination. When analysing Figure 1a, one can see that, as increases from 200 to
The
observed combination of strength and ductility characteristics was caused by
the structural state of steel, formed in the process of accelerated cooling and
during subsequent self-tempering. The conducted electron microscopic studies of
the wheel disc metal showed that the identified substructural peculiarities
qualitatively coincided with results reported in similar studies on carbon
steels subjected to accelerated cooling [11].
a b
Fig. 1. The changes in
the steel properties due to the temperature of the accelerated cooling
termination. Strength (a): (♦), (■); and plastic (b): d (♦), y (■) (the characteristics)
It
transpires that the mechanical properties of the studied steel, when rapidly
cooled to 200-300оС, are largely similar to the
properties after martensite quenching (with separate heating) and tempering at
these temperatures [9,10]. Figure 2 shows the structure of steel after
accelerated cooling to 200-250оС. The analysis presented
in this figure shows the presence of not only upper and lower bainite (Figure
2a-b), but also the eutectoid colonies of high dispersion (Figure 3a-b). The
differences between the volumes of lower and upper bainite are found in the
morphological features of the carbide phase structure. For upper bainite, the
characteristic feature is the presence of relatively large elongated cementite
particles (Figure 2a), with a primary location along the lath borders of the a-phase. The areas of lower bainite are the
metal volumes with dispersed carbide particles located within the lathes
(Figure 2b). In this case, the observed image clarity reduction in the lath
borders of lower bainite in some microvolumes indicates the increased density
of dislocations in the a-phase. The growth in the distance
from the cooling surface is accompanied by certain structural changes, starting
from the bainitic structures near the disc surface to the ferrite-pearlite
phase components with different dispersion and morphology. Compared to the
metal located near the surface of intensive cooling (Figure 2), in the volumes
lying in the central part of the wheel disc, the microstructure is formed
mainly according to the diffusion mechanism (Figure 3). This is indicated by a
finely differentiated pearlite structure and the areas of structurally free
ferrite located at the boundaries of the pearlite colonies (Figure 3a). The
thickness of cementite plates in pearlite is about 0.02-0.04 μ, while the
thickness of ferrite layers is no more than 0.15 μ. The morphology change
in the carbide phase, starting from thin intermittent plates to dispersed
particles of a globular form, shows that the metal is heated to different
temperatures after the accelerated cooling termination.
a b
Fig. 2. The microstructure of steel
after accelerated cooling to 200-250°C:
upper bainite (a), lower bainite (b) (magnification: 18,000)
During
detailed analysis, the division of areas of structurally free ferrite (Figure
3b) into subgrains with dimensions of 1.5-3.5 μ can be found. The form of
subgrains varies from a polyhedron with a high dislocation density to
needle-like formations. The presence of ferrite of a different morphology is
explained by differences in cooling rates due to disc thickness and the possible
liquation of chemical elements in the metal microvolumes [8].
A further
increase in the temperature of the accelerated cooling termination to 400°C is
followed by the somewhat expected qualitative changes in the microstructure.
The formation of complex dislocation tangles, which occur as broken contours in
the dislocation complexes, corresponds to the occurrence of signs of the
development of polygonization processes (Figure 4a). In other microvolumes of
ferrite, the presence of cementite particles of a globular form is observed
within the areas with a low dislocation density (Figure 4b). This fact
indicates the completion of polygonization. The simultaneous behaviour of these
processes leads to the formation of a rather complex modulated structure. Individual
cells, with a specific dislocation density inside them, are sufficiently
separated from wide dislocation walls (Figure 4b). In general, the formed
cellular dislocation structure resembles a polyhedral form; the central part of
the cells is largely cleared from unbound dislocations. However, a certain
number of cementite particles, with sizes greater than that after
self-tempering at 200°C, can be found in the structure. Thus, the nature of the
influence of the self-tempering temperature increase on the metal structure is
based on the progressive reduction in the degree of solid solution
supersaturation by carbon atoms, the increase of the average size of carbide
particles and the recombination of dislocations reducing their density.
a b
Fig. 3. The
microstructure of metal in the axial part of the disc (magnification: 12,000)
The
structural state of railway wheel disc steel near the surface of accelerated
cooling is caused by the development of bainite transformation with
self-tempering in the temperature range 200-300оС, which
leads to the achievement of the level of strength properties as follows:
1,320-1,200 MPa [4].
A
detailed analysis of structural changes from the temperature of the accelerated
cooling termination () indicates the development of two
competing processes: reducing the degree of solid solution supersaturation by
carbon atoms and dispersion hardening from the carbide phase particles. The
nature of the microhardness change () of the ferrite component shows that,
with an increase in the temperature of the accelerated cooling termination
(starting from 200оС), a continuous decrease in the
concentration of carbon atoms in the solid solution is observed (Figure 5a). On
this basis, it should be assumed that the development of steel softening
processes with the tt increase will, to a greater extent, depend on
the carbon atoms’ transfer from the solid solution to the defects in the
crystal structure than on the contribution of the dispersion strengthening of
ferrite. On the basis of the angular coefficient of dependence , the reduction degree in solid
solution supersaturation by carbon atoms can be qualitatively judged. At the
same time, ferrite has a sufficiently high density of crystalline structure
defects, especially the dislocations, as evidenced by the change behaviour of
the line width of the X-ray interference of ferrite (Figure
5b.). The comparison of microhardness values (Figure 5a) and makes it possible to determine the intervals
with a qualitatively different nature of structural changes in the metal during
self-tempering. It is supposed that, at the temperature of self-tempering,
i.e., 350°C, the point of almost full exhaustion of the evolution resource of
carbon atoms from the solid solution on dislocations (acceleration of a
reduction in the values and at temperatures above 350°C) is
achieved.
a b
Fig. 4. The
microstructure of steel after accelerated cooling to 400°C (magnification:
18,000)
Similar
results were obtained when analysing the nature of hardening for most of the
mix of rolled stock after accelerated cooling. In [9,10], it is shown that,
starting from temperatures of 350оС and above, in the
structure of carbon steel, one can already find a certain number of fine
particles of the carbide phase. On this basis, the carbon depletion of the
solid solution will take place due to the direct diffusion of carbon atoms from
the solid solution for carbide particles, which, to some extent, is confirmed
by the change nature of the metal strength properties (Figure 1a). A detailed
analysis of the curve rate indicates that the main factor of hardening during
accelerated cooling is the degree of solid solution supersaturation by carbon
atoms, while the dispersion strengthening has a lesser influence. On the other
hand, the process of carbon depletion of the solid solution has a dual nature
of influence on the strength properties. The evolution of carbon atoms from the
octahedral interstices in the crystalline lattice of ferrite on dislocation,
which contributes to their further consolidation [9], leads to hardening. At
the same time, a reduction in the concentration of carbon atoms in the solid
solution, which leads to softening, further increases the amount of dispersed
cementite particles. Dispersion hardening from these particles will enhance the
strength characteristics of the metal. On the other hand, the transition of the
carbon atoms from the solid solution to the carbide particles is accompanied by
a reduction in internal stresses, which is evidenced by an increase in the
contrast of the reflexes of microdiffraction images [7, 10] and a reduction in
the broadening of X-ray ferrite interferences (Figure 4b).
At higher
temperatures of the accelerated cooling termination, a progressive decrease is
observed in the ferrite microhardness and the corresponding decrease in the
value of , alongside well-defined qualitative
changes in the internal structure of the metal corresponding to them. As the
temperature increases to 400-450оС, the intensive
development of the polygonization process is started, especially in the areas
of bainite.
a b
Fig. 5. Influence of the
accelerated cooling end temperature on ferrite microhardness
(a) and the b(110) of ferrite (b)
The
formation of cells of a polygonal form is accompanied by the emergence of
boundaries with a different degree of perfection. In the middle of the cells,
the dislocation density is significantly reduced, compared to the lower
temperature of the cooling termination. In some microvolumes, the metal
redistribution of dislocations leads to the initial stages of the “spillage” of
boundaries with small angles of disorientation. In the pearlite colonies, the
spheroidization and coalescence of cementite are accelerated. The simultaneous
development of these phenomena explains the observed change behaviour in the
property complex of wheel disc metal at different distances from the surface of
accelerated cooling (Figure 1). According to these results, the effect of
softening from reducing the degree of solid solution supersaturation by carbon
atoms, as well as reducing the dislocation density and coalescence of cementite
particles, exceeds the strengthening effect from the presence of fine carbide
particles in the structure.
Thus, the
accelerated cooling termination at temperatures of up to 300°C, the level of
steel strength properties is determined by the combined effect from the processes
of carbon atoms’ evolution from the solid solution for dislocations and
dispersion hardening of cementite from the formation of an additional quantity
of cementite particles. The analysis of the obtained results indicates that the
use of accelerated cooling of the disc to 350-400⁰С, when manufacturing the all-rolled railway wheel, will make it
possible to improve the strength characteristics of metal without reducing the
ductility properties, as compared to air cooling. The existing regulatory
requirements (Standard EN 13262: 2004, Steel ER 9) confirm the relevance of
technical solutions aimed at improving the strength properties of the railway
wheel disc.
4. CONCLUSIONS
Firstly, accelerated cooling of the surface of the
railway wheel disc to a temperature in the range of 350-400оС
enhances the strength characteristics of the metal, as compared to cooling in
air. Secondly, the level of strength properties of the metal disc is regulated
by the temperature of the accelerated cooling termination after achieving the
desired effect from the development of hardening and softening processes.
Acknowledgements
The authors would like to express
their gratitude to D Assoc. O.A. Tchaikovsky for their valuable advice given
during the discussion of our results.
References
1. Vakulenko I.О., O.M.
Perkov, D.M. Bolotova, S.V. Proydak. 2015. “A method of manufacturing a
complete rim of a railway wheel”. Patent for the Corsna Model. No 96845. 25
February 2015. Bul. No 4. Ukraine.
2. Vakulenko I.A., N.A. Grishenko. 2010.
“Structural changes in a railway wheel rim during operation”. Russian Metallurgy 5: 408-411.
3. Vakulenko I.O. 2016.
“Influence of cooling rate on the strength of the rims of railway wheel”. Materials Science 51(6): 839-842.
5. Vakulenko
I.O., V.H. Anofriyev, M.A. Hryshchenko, O.M. Perkov. 2009. Defects of Railway Wheels. Makovetsky, Ukraine: DK.
6. Efremenko
VG., F.K. Tkachenko, S.O. Kuzmin et al. 2009. “Kinetics of transformation of
austenite in rail steels of brands M74 and 75HGSM with continuous cooling”. Вісн.
Дніпропетр. nat.
un-tu hall. transp. ім. acad. V. Lazaryan 29: 198-201.
7. Kuz’min
S.O., V.G. Efremenko, Y.G. Chabak, E.V. Tsvetkova.
2013. “Morphologic features of bainite in high-carbon complex-alloyed steel”. Metallofizika i
Noveishie Tekhnologii 35(9): 1271-1282.
8. Bhadeshia H.K.D.H. 2001. Bainite in Steels. Cambridge: Cambridge
University Press.
9.
Vakulenko I., O. Perkov, N.
Grishchenko. 2009. “Optimal structural state of metal for railroad wheels and
rails”. Stahl und Eisen 9.
10. Vakulenko I.A. 2008. Morphology of Structure and Strain Hardening
of Steel. Makovetsky, Ukraine: DK.
11. Bolshakov
V.I., G.D. Sukhomlin, N.E. Pogrebnaya N.E. 2001. Atlas of Structures of Metals and Alloys. Dnepropetrovsk, Ukraine:
Gaudeamus.
12. Efimova,
О.Y., Y.F. Ivanov, S.V. Konovalov, V.E. Gromov. 2011. “Gradient
structural-phase states in the thermostrengthened low-carbon steel
reinforcement”. Materials and
Manufacturing Processes 26(1): 144-146.
Received 09.10.2017; accepted in revised form 15.02.2018
Scientific Journal of
Silesian University of Technology. Series Transport is licensed under
a Creative Commons Attribution 4.0 International License
1 Dnipropetrovsk National University
of Railway Transport Named After Academician V. Lazaryan, Lazaryan St., 2,
Dnipro, Ukraine, 49010. E-mail: dnuzt_texmat@ukr.net.
2 Dnipropetrovsk National University
of Railway Transport Named After Academician V. Lazaryan, Lazaryan St., 2,
Dnipro, Ukraine, 49010. E-mail: grichenko@live.ru.
3 Management of the
Pridniprovsk Railway, D. Yavornizkogo Av., 108, Dnipro, Ukraine, 49600. E-mail:
dnuzt_texmat@ukr.net.
4 Pryazovskyi State
Technical University, Mariupolskay St., 7, Mariupol, Ukraine, 87500. E-mail:
vgefremenko@mail.ru.
5 Dnipropetrovsk National University
of Railway Transport Named After Academician V. Lazaryan, Lazaryan St., 2,
Dnipro, Ukraine, 49010. E-mail: proydak.s@gmail.com.
6 Iron and Steel Institute,
Starodubov Sq., 1a, Dnipro, Ukraine, 49107. E-mail: dnuzt_texmat@ukr.net.